Marvel Team-Up Vol. 1 #83

Plot

Guest-starring Spider-Man, Nick Fury, and the Black Widow. In stunning fashion, the web-slinger and the widow have gone down to defeat at the hands of SHIELD and its director, Nick Fury! Now the Black Widow is a prisoner of SHIELD, and a dazed Spider-Man is trying to figure out what is going on. When Natasha escapes from the SHIELD facility, she turns to her only friend left in Manhattan...Peter Parker! At his Chelsea apartment, Aunt May's nephew is consoling Natasha, when all of a sudden Nick Fury kicks in the door! Minutes later Boomerang attacks! And then the Silver Samurai! It's a wild free-for-all in the streets with the wall-crawler and the Black Widow caught in the middle! (mycomicshop.com)